TGA, MS and DSC of a solid polymeric Ge hydride, obtained by γ-radiolysis of GeH4, are reported. Upon heating, it undergoes two successive weight losses at 463 and 1173 K. At 948 K two crystal phases are formed, one of them is pure germanium. Some comparisons with a-Ge: H produced via RF sputtering or glow discharge are reported.
Thermolysis and mass spectra of polymeric germanium hydride produced by -radiolysis
BENZI, Paola;CASTIGLIONI, Mario;VOLPE, Paolo Edoardo Angelo;BATTEZZATI, Livio;
1988-01-01
Abstract
TGA, MS and DSC of a solid polymeric Ge hydride, obtained by γ-radiolysis of GeH4, are reported. Upon heating, it undergoes two successive weight losses at 463 and 1173 K. At 948 K two crystal phases are formed, one of them is pure germanium. Some comparisons with a-Ge: H produced via RF sputtering or glow discharge are reported.
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